Inductively Coupled Plasma-Mass Spectrometry

Practices and Techniques

By: Howard E. Taylor

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Hardcover | 17 October 2000

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Inductively Coupled Plasma-Mass Spectrometry presents a concise A-Z description of inductively coupled plasma-mass spectrometry, written in layman's terms, for use in the solution of trace element analytical chemistry problems. Detailed discussion of sample introduction and data interpretation is provided.

Practicing analytical chemists will be able to use this text to familiarize themselves with the principles, approaches, options, pitfalls, and advantages of ICP-MS technology.

Key Features
* Concise and straightforward descriptions of ICP-MS principles and instrumentation, ensuring rapid understanding of the technique and its advantages and limitations
* Examples to clarify the operational characteristics of the technology
* Drawings and illustrations to clarify principles, techniques, and methodology
* Discussions of practical approaches to the solution of specific trace analysis problems with helpful tips on efficiently producing the most accurate and precise data
* Easy-to-understand terms, so that new users of the technology will immediately benefit from the information provided
* Comprehensive appendixes containing isotopic and interference data
* An exhaustive compilation of literature citations for supplemental information

Industry Reviews

"The Editor, Professor Steve Hill, states in the preface that the purpose was to produce a book that covers both theory and applications in a concise, informative and readable form. This has certainly been achieved and the book is a very welcome addition to the literature." "...The content is excellent. I am very pleased to have a copy of this book for my own use and it would be amongst my first-choice texts to recommend to students or those who have little or no previous experience of plasma source spectrometry." --B. L. Sharp, Department of Chemistry, Loughborough University, TRENDS IN ANALYTICAL CHEMISTRY,Vol.19, No.8, August 2000 "...well-written and easy to read...a good introduction to ICP-MS." --John W. Olesik, Ohio State Univ., Journal of American Society of Mass Spectrometry

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About the Author	p. xi
Introduction
History	p. 2
Overview	p. 3
Atomic Structure
Bohr Model	p. 8
Isotopes	p. 10
Ionization	p. 11
Inductively Coupled Plasmas
Plasma Formation	p. 16
Generators	p. 17
Crystal-Controlled Oscillator	p. 17
Free-Running Oscillator	p. 18
Solid-State Generators	p. 19
Load Coils	p. 20
Torches	p. 20
Plasma Configuration	p. 23
Instrumentation
Interface	p. 30
Ion Lenses	p. 31
Mass Spectrometers	p. 34
Quadrupole Mass Analyzer	p. 34
Scanning	p. 36
Peak Hopping	p. 38
Resolution	p. 38
Abundance Sensitivity	p. 39
Magnetic Sector Mass Analyzer	p. 40
Single Focusing	p. 40
Double Focusing	p. 41
Time-of-Flight Mass Spectrometer	p. 44
Ion-Trap Mass Spectrometer	p. 46
Detectors	p. 47
Continuous Dynode Electron Multiplier	p. 47
Discrete Dynode Electron Multiplier	p. 49
Faraday Cup	p. 50
Sample Introduction
Gaseous Samples	p. 55
Vapor Generation	p. 56
Hydride Generation	p. 56
Osmium Tetroxide Vapor	p. 58
Cold-Vapor Mercury	p. 60
Chromatography	p. 60
Vapor Phase Chromatography	p. 60
Supercritical Fluid Chromatography	p. 62
Liquid Samples	p. 62
Nebulizers	p. 63
Spray Chamber	p. 64
Pneumatic Nebulizer	p. 67
Ultrasonic Nebulizer	p. 73
Electrothermal Vaporizers	p. 76
Solid Samples	p. 79
Ablation Methods	p. 81
Laser Ablation	p. 81
Spark Ablation	p. 85
Slurry Nebulization	p. 87
Direct Insertion	p. 88
Special Techniques
Flow Injection	p. 91
Chromatography	p. 95
Liquid Chromatography	p. 95
Ion-Exchange Chromatography	p. 97
Field Flow Fractionation	p. 98
Quantitation Techniques
Qualitative Analysis	p. 104
Semiquantitative Analysis	p. 106
Quantitative Analysis	p. 108
Direct Calibration	p. 109
Calibration Curves	p. 109
Internal Standardization	p. 112
Standard Addition	p. 115
Isotope Dilution	p. 117
Quantitation Strategy	p. 122
Interferences
Spectrometric Effects	p. 126
Isobaric Spectral Overlap	p. 126
Polyatomic Molecular Spectral Overlap	p. 128
Polyatomic Molecules from Plasma Gas Components	p. 129
Molecular Oxides	p. 129
Sample Matrix/Acid Components	p. 131
Reaction/Collision Cells	p. 134
Doubly Charged Ions	p. 136
Background	p. 136
Nonspectrometric Effects	p. 137
Matrix Effects	p. 137
Physical Effects	p. 139
Optimization
Parameter Optimization	p. 144
"Cold Plasma" Operating Conditions	p. 147
Figures of Merit
Sensitivity	p. 150
Detection Limits	p. 151
Precision	p. 155
Accuracy	p. 157
References	p. 161
Table of Elements with Atomic Number, Weights, and First and Second Ionization Potentials	p. 163
Isotopic Composition of the Elements	p. 167
Prominent Polyatomic Interferences Applicable for ICP-MS Determinations	p. 175
Table of Student's t Distribution	p. 179
Certified Standard Reference Materials Available from the U.S. NIST and the NRC of Canada	p. 181
Supplemental References	p. 187
Index	p. 289
Table of Contents provided by Syndetics. All Rights Reserved.

Inductively Coupled Plasma-Mass Spectrometry

Practices and Techniques

Industry Reviews

Shipping

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