NMR in Supramolecular Chemistry

By: Miquel Pons (Editor)

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Hardcover | 31 March 1999

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NMR is better suited than any other experimental technique for the characterization of supramolecular systems in solution. The presentations included here can be broadly divided into three classes. The first class illustrates the state of the art in the design of supramolecular systems and includes examples of different classes of supramolecular complexes: catenanes, rotaxanes, hydrogen-bonded rosettes, tubes, capsules, dendrimers, and metal-containing hosts. The second class comprises contributions to NMR methods that can be applied to address the main structural problems that arise in supramolecular chemistry. The third class includes biological supramolecular systems studied by state-of-the-art NMR techniques.

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Organizing Committee
Foreword
List of Participants
Probing Self-Assembly by NMR	p. 1
Study of Conformational Behavior of CMP(O)-Cavitands by NMR Spectroscopy and X-Ray Analysis in Relation to the Extraction Properties	p. 19
NMR Studies of Molecular Recognition by Metalloporphyrins	p. 37
Reversible Dimerization of Tetraureas Derived from Calix[4]arenes	p. 45
Self-Assembling Peptide Nanotubes	p. 61
Symmetry: Friend or Foe?	p. 67
Quenching Spin Diffusion in Transferred Overhauser Studies and Detection of Octupolar Order in Gaseous Xenon-131	p. 83
Applications of NMR Spectroscopy to the Study of the Bound Conformation of O- and C-Glycosides to Lectins and Enzymes	p. 99
Application of NMR to Conformational Studies of an HIV Peptide Bound to a Neutralizing Antibody	p. 117
Paramagnetic NMR Effects of Lanthanide Ions as Structural Reporters of Supramolecular Complexes	p. 133
Characterization of Reaction Complex Structures of ATP-Utilizing Enzymes by High Resolution NMR	p. 155
Spin Relaxation Methods for Characterizing Picosecond-Nanosecond and Microsecond-Millisecond Motions in Proteins	p. 171
Structural Diversity of the Osmoregulated Periplasmic Glucans of Gram-Negative Bacteria by a Combined Genetics and Nuclear Magnetic Resonance Approach	p. 191
NMR Studies of the 269 Residue Serine Protease PB92 from Bacillus Alcalophilus	p. 227
Intermolecular Interactions of Proteins Involved in the Control of Gene Expression	p. 247
NMR-Based Modeling of Protein-Protein Complexes and Interaction of Peptides and Proteins with Anisotropic Solvents	p. 255
Protein Surface Recognition	p. 267
NMR Studies of Protein-Ligand and Protein-Protein Interactions Involving Proteins of Therapeutic Interest	p. 281
NMR Diffusion Measurements in Chemical and Biological Supramolecular Systems	p. 301
Determination of Calixarene Conformations by Means of NMR Techniques	p. 307
Structure, Molecular Dynamics, and Host-Guest Interactions of a Water-Soluble Calix[4]arene	p. 311
Cation Complexation and Stereochemistry of Macrocycles Studied by [superscript 13]C NMR Relaxation-Time Measurements	p. 315
A Comparative Study on Liquid State CSA Methods	p. 319
Hydrogen Bonding and Cooperativity Effects on the Assembly of Carbohydrates	p. 325
Influence of Substituents on the Edge-to-Face Aromatic Interaction: Halogens	p. 331
Subject Index	p. 335
Table of Contents provided by Blackwell. All Rights Reserved.

NMR in Supramolecular Chemistry

At a Glance

Hardcover

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