Square-Wave Voltammetry

Theory and Application

By: Valentin Mirceski, Sebojka Komorsky-Lovric, Milivoj Lovric

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Hardcover | 14 November 2007

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212 Pages

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23.39 x 15.6 x 1.27

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Square-wave voltammetry is a technique readily available to every researcher, scientist, engineer and practitioner applying modern electrochemical measurement systems. It is of beneficial use in analytical applications and in fundamental studies of electrode mechanisms. But the optimised exploitation of this technique is only possible for those with a detailed knowledge of signal generation and of the thermodynamics and kinetics involved. This volume, written by three distinguished experts, systematically delivers the complete and in-depth information that enables both researchers and users of square-wave voltammetry to apply this technique effectively. Square-Wave Voltammetry also offers an appendix on mathematical modeling and a chapter on the most important electrode mechanisms which briefly reviews the underlying theory and numerical formulae intrinsic for simulating experiments with popular software tools , e.g. Mathcad (R).

Industry Reviews

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"This book provides a wide collection of data for the description of diverse tendencies that characterize several electrochemical reactions analyzed by SWV. ... In summary, the book is highly recommended for researchers and research students who are interested in working with SWV. The authors are some of the foremost experts on the computation and experimental studies about this technique ... . the authors provide an excellent introduction for anybody interested in the simulation of voltammetric curves." (Fernando Garay, Journal of Solid State Electrochemistry, Vol. 13, 2009)

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Introduction	p. 1
From Square-Wave Polarography to Modern Square-Wave Voltammetry	p. 1
Square-Wave Voltammetry: Calculations and Instrumentation	p. 6
References	p. 11
Electrode Mechanisms	p. 13
Electrode Reactions of Dissolved Species on Stationary Planar Electrodes	p. 13
Reversible Electrode Reactions	p. 13
Kinetically Controlled Electrode Reaction	p. 17
Reactions of Dissolved Species on Spherical Electrodes and Microelectrodes	p. 25
Reactions of Amalgam-Forming Metals on Thin Mercury Film Electrodes	p. 32
Reversible Reduction of Metal Ions on Stationary Electrode	p. 32
Anodic Stripping Square-Wave Voltammetry of Metal Ions	p. 35
Chemical Reactions Coupled to Electrode Reactions	p. 39
CE Mechanism	p. 40
EC Mechanism	p. 45
ECE Mechanism	p. 49
EC' Catalytic Mechanism	p. 54
Surface Electrode Reactions	p. 60
Simple Surface Electrode Reaction	p. 60
Surface Electrode Reaction Involving Interactions Between Immobilized Species	p. 77
Surface Electrode Reactions Coupled with Chemical Reactions	p. 81
Two-Step Surface Electrode Reaction	p. 91
Mixed-Electrode Reactions	p. 97
Electrode Reactions Coupled with Adsorption of the Reactant and Product of the Electrode Reaction	p. 97
Electrode Reactions Coupled with Adsorption and Chemical Reactions	p. 110
Electrode Reactions of Insoluble Salts	p. 121
Square-Wave Voltammetry Applied to Thin-Layer Cell	p. 130
References	p. 139
Applications	p. 143
Quantitative Analysis	p. 143
Qualitative Identification of Phases	p. 149
Mechanistic and Kinetic Studies	p. 150
References	p. 157
Square-Wave Voltammetry at Liquid-Liquid Interface	p. 163
Three-Phase Electrodes and Their Application to Measure the Energy of Ion Transfer Across Liquid-Liquid Interface	p. 163
Analyzing the Kinetics of the Ion Transfer Across Liquid-Liquid Interface with Thin-Film Electrodes	p. 169
References	p. 177
Mathematical Modeling of Electrode Reaction in a Thin-Layer Cell with the Modified Step-Function Method	p. 179
References	p. 185
Index	p. 197
Table of Contents provided by Ingram. All Rights Reserved.

Square-Wave Voltammetry

Theory and Application

At a Glance

Hardcover

Industry Reviews

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Paperback

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